原著論文リスト



1990
  1. Asakura,Tetsuo., Yoshimizu, Hiroaki. and Kakizaki, Mitsuhiro., An Esr Study ofSpin-Labeled Silk Fibroin Membranes and Spin-Labeled Glucose-OxidaseImmobilized in Silk Fibroin Membranes, Biotechnol. Bioeng., 35-5,511-517, 1990.
  2. Asakura,Tetsuo., Yamada, Hiroyuki., Demura, Makoto. and Osanai, Minoru., 13Cand 31P Nmr Analyses of the Cultured Posterior Silk Gland of theSilkworm, Bombyx-Mori - Silk Fibroin Production and the Effect ofSorbitol-6-Phosphate, Insect Biochem, 20-3, 261-266, 1990.
  3. Yoshimizu,Hiroaki. and Asakura, Tetsuo., Preparation and Characterization of Silk FibroinPowder and Its Application to Enzyme Immobilization, J. Appl. Polym. Sci,40-1-2, 127-134, 1990.
  4. Yoshimizu,Hiroaki. and Asakura, Tetsuo., The Structure of Bombyx-Mori Silk FibroinMembrane Swollen by Water Studied with Esr, C-13-Nmr, and Ft-Ir Spectroscopies,J. Appl. Polym. Sci, 40-9-10, 1745-1756, 1990.
  5. Saito,Hazime., Ishida, Mika., Yokoi, Motoko. and Asakura, Tetsuo., Dynamic Featuresof Side-Chains in Tyrosine and Serine Residues of Some Polypeptides andFibroins in the Solid as Studied by High-Resolution Solid-State C-13Nmr-Spectroscopy, Macromolecules, 23-1, 83-88, 1990.
  6. Ishida,Mika., Asakura, Tetsuo., Yokoi, Motoko. and Saito, Hazime., Solvent-Induced andMechanical-Treatment-Induced Conformational Transition of Silk Fibroins Studiedby High-Resolution Solid-State C-13 Nmr-Spectroscopy, Macromolecules, 23-1,88-94, 1990.
  7. Yamamoto,Ryota., Araki, Kazuo., Imamura, Yoshio., Asakura, Tetsuo., Iizuka, Eisaku. andIida, Shuji., C-13 Nmr-Studies of Thermotropic Liquid-Crystalline Poly(Gamma-AlkylarylL-Glutamate)S, Makromol. Chem, 191-2, 345-354, 1990.
  8. Lenka,Subasini., Demura, Makoto. and Asakura, Tetsuo., C-13 Nmr-Studies of thePolymerization Mechanism and the Dynamics of Poly(AlkylMethacrylate) Grafted onto Silk Fibers, Makromol. Chem, 191-6,1321-1327, 1990.
  9. Yamamoto,Ryota., Araki, Kazuo., Imamura, Yoshio., Iimura, Kazuyoshi., Asakura, Tetsuo.and Iizuka, Eisaku., Molecular Side-Chain Motion and Its Free-Volume inThermotropic Liquid-Crystalline Poly(Gamma-AlkoxybenzylL-Glutamate)S Using Spin Probe Electron-Paramagnetic Resonance, Makromol.Chem., Rapid commun, 11-6, 293-298, 1990.
  10. Ando,Isao., Yamanobe, Takeshi and Asakura, Tetsuo., Primary and Secondary Structuresof Synthetic-Polymer Systems as Studied by 13C Nmr-Spectroscopy,Prog. Nucl. Magn. Reson. Spectrosc, 22, 349-400, 1990.
  11. 出村誠, 香村恭史, 平出啓 and 朝倉哲郎, リパーゼ固定化絹フィブロイン膜の酵素性能とその膜電位応答性, 繊維学会誌, 46-9,391-396, 1990.
  12. □朝倉哲郎, 出村誠, グルコースセンサーへの不織布の応用, バイオインダストリー,1990, 7, 676-682
  13. □朝倉哲郎, 絹の体外生産, 高分子,1990, 39, 523
  14. □朝倉哲郎, 絹研究最前線, バウンダリー,1990, 6, 49-57
  15. □朝倉哲郎, 繊維の女王, 絹の大変身, おもしろいバイオ新素材のはなし, 松永是, 本宮達也編著, 日刊工業新聞,1990, 23-33



1991
  1. Demura,Makoto., Komura, Takashi. and Asakura, Tetsuo., Membrane-Potential of Bombyx-MoriSilk Fibroin Membrane Induced by an Immobilized Enzyme Reaction,Bioelectrochem. Bioenerg., 26-2, 167-175, 1991.
  2. Asakura,Tetsuo., Demura, Makoto., Nagashima, Mariko., Sakaguchi, Ryuji., Osanai,Minoru. and Ogawa, Katsuaki., Metabolic Flux and Incorporation of[2-C-13]Glycine into Silk Fibroin Studied by C-13 Nmr Invivo and Invitro,Insect Biochem, 21-7, 743-748, 1991.
  3. 朝倉哲郎, 北口源啓, 出村誠, 酒井治利, 金子正夫, 栗岡聡 and 小松計, 「不織布表面にコーティングされたスピンラベルグルコースオキシダーゼならびにスピンラベル絹フィブロインのESR解析」, J.Seric.Sci.Jpn, 60-6,466-474, 1991.
  4. Asakura,Tetsuo., Nakamura, Eiji., Asakawa, Harumi. and Demura, Makoto., Ring-CurrentEffects and Magnetic-Anisotropy Effects of Carbonyl Groups on the Alpha-ChProton Chemical-Shifts of the Basic Pancreatic Trypsin-Inhibitor andTendamistat,  J Magn Reson, 93-2, 355-360, 1991.
  5. Williamson,Michael P. and Asakura, Tetsuo., Calculation of Chemical-Shifts of Protons onAlpha Carbons in Proteins, J Magn Reson, 94-3, 557-562, 1991.
  6. Demura,Makoto. and Asakura, Tetsuo., Porous Membrane of Bombyx-Mori SilkFibroin - Structure Characterization, Physical-Properties and Application toGlucose-Oxidase Immobilization, J.Membrane Sci., 59-1, 39-52, 1991.
  7. Kaneko,Masao., Iwahata, Shinichi. and Asakura, Tetsuo., Luminescence Form Excited Tris(2,2'-Bipyridine)-Ruthenium(Ii)Incorporated into a Silk Fibroin Membrane, J. Photochem. Photobiol. A, 61-3,373-380, 1991.
  8. Asakura,Tetsuo., Demura, Makoto., Ogawa, Hidejiro., Matsushita, Kazuhiro. and Imanari,Mamoru., NMR imaging of diffusion of small organic molecules in silk fibroingel, Macromolecules, 24-2, 620-622, 1991.
  9. Asakura,Tetsuo., Demura, Makoto. and Nishiyama, Yuko., 13C Nmr SpectralAssignment of 5 Polyolefins Determined from the Chemical-Shift Calculation andthe Polymerization Mechanism, Macromolecules, 24-9, 2334-2340, 1991.
  10. Yoshimizu,Hiroaki., Asakura, Tetsuo. and Kaneko, Masao., Luminescent Characteristics ofTris(2,2'-Bipyridine)-Ruthenium(Ii)Adsorbed in a Silk Fibroin Membrane, Makromol. Chem, 192-7, 1649-1654,1991.
  11. Asakura,Tetsuo., Hirano, Koki., Demura, Makoto. and Kato, Kazuya., 2D-in Adequate 13CNmr-Spectra of Atactic Polyolefins, Makromol. Chem., Rapid commun, 12-4,215-220, 1991.
  12. Asakura,Tetsuo. and Nakayama, Nobuhiko., C-13 Nuclear-Magnetic-Resonance Analysis ofPoly(3-Methyl-1-Butene),Polymer Comm, 32-7, 213-216, 1991.
  13. □安藤勲, 朝倉哲郎, 高分子化学,“実験化学講座5巻｢NMR｣”(荒田洋治編),1991, 丸善,261-296



1992
  1. Demura,Makoto., Takekawa, Toshihiro., Asakura, Tetsuo. and Nishikawa, Akihumi.,Characterization of Low-Temperature-Plasma Treated Silk Fibroin Fabrics by Escaand the Use of the Fabrics as an Enzyme-Immobilization Support,Biomaterials, 13-5, 276-280, 1992.
  2. Williamson,Michael P. and Asakura, Tetsuo., The Application of H-1-Nmr Chemical-ShiftCalculations to Diastereotopic Groups in Proteins, FEBS Lett., 302-2,185-188, 1992.
  3. 出村誠, 竹之下仁子, 朝倉哲郎, 酒井治利, 栗岡聡, 小松計一 and 金子正夫, 「絹セシリン / 絹フィブロインブレンドコーティングによる酵素固定化不織布」, J.Seric.Sci.Jpn, 61-1,66-72, 1992.
  4. Asakura,Tetsuo, Kitaguchi, Motohiro, Demura, Makoto, Sakai, Harutoshi and Komatsu,Keiichi, Immobilization of glucose oxidase on nonwoven fabrics with Bombyxmori silk fibroin gel, J. Appl. Polym. Sci, 46-1, 49-53, 1992.
  5. Williamson,Michael P., Asakura, Tetsuo., Nakamura, Eiji. and Demura, Makoto., A Method forthe Calculation of Protein Alpha-Ch Chemical-Shifts, J. Biomol. NMR, 2-1,83-98, 1992.
  6. Asakura,Tetsuo., Niizawa, Yoshimi. and Williamson, Michael P., Determination of theMagnetic-Anisotropy of the Oxygen Atom and H-1 Chemical-Shift Calculation ofProteins, J Magn Reson, 98-3, 646-653, 1992.
  7. Asakura,Tetsuo., Demura, Makoto., Watanabe, Yasuo. and Sato, Kazuo., H-1 PulsedNmr-Study of Bombyx-Mori Silk Fibroin - Dynamics of Fibroin and ofAbsorbed Water, J Polymer Sci B Polymer Phys, 30-7, 693-699, 1992.
  8. 朝倉哲郎, 出村誠, 中村英二 and 安藤勲,Basic Pancreatic Trypsin Inhibitorのα-CH及びNH 1HNMR化学シフトの理論的計算,Kobunshi Ronbunshu, 49-4, 281-287, 1992.
  9. Aoki,Akira., Hayashi, Tetsuo. and Asakura, Tetsuo., C-13 Nmr Chemical-ShiftAssignments of Comonomer Sequences in a 1-Butene Propylene Copolymer,Macromolecules, 25-1, 155-160, 1992.
  10. Asakura,Tetsuo., Nakayama, Nobuhiko., Demura, Makoto. and Asano, Atsushi., C-13 Nmr SpectralAssignments of Regioirregular Polypropylene Determined from 2-DimensionalInadequate Spectra and Chemical-Shift Calculations, Macromolecules, 25-19,4876-4881, 1992.
  11. Kaneko,Masao, Takekawa, Toshihiro and Asakura, Tetsuo, Photoluminescent copolymer-pendantRu(BPY)32+grafted onto non-woven silk fabric and its application to oxygen sensor,Makromol Chem Macromol Symp, 59-1, 183-197, 1992.
  12. Kaneko,Masao., Iwahata, Shinichi. and Asakura, Tetsuo., Quenching of Photoexcited 4,4'-Dicarboxy

    -2,2'-Bipyridinebis(2,2'-Bipyridine)Ruthenium(Ii)by Oxygen in Aqueous-Solution and in Silk Fibroin Membrane, Photochem.Photobiol., 55-4, 505-509, 1992.
  13. Asakura,Tetsuo. and Nakayama, Nobuhiko., 2D-Inadequate 13CNuclear-Magnetic-Resonance Assignment of Regioirregular Poly(1-Butene),Polymer, 33-3, 650-654, 1992.
  14. □朝倉哲郎, コンフォメーション, 高分子と生体高分子のNMR(中條利一郎ら編), 東京化同人,1992, 79-92
  15. □朝倉哲郎, 出村誠, 絹の新しい利用とカイコ体外での生産, 高分子化工1992,41, 442-446
  16. □Horii, F .; Nakagawa, M .; Kitamaru, R .; Chujo, R.; Hatada, K .; Tanaka, Y .; Amiya, S .; Asakura, T .; Chikaishi, K. ; Goto, Y.; Hikichi, K .; Hirakida, Y. ; Hosoda, S .; Imanari, M .; Itoh, S .; Kamachi,M .; Kawamura, T .; Kitayama, T .; Kohjiya, S .; Lee, K .; Nagoya, I .; Oka, Y.; Okada, T .; Okumura, M .; Saito, T .; Sato, H .; Sei, T .; Seimiya, T .;Shiibashi, T .; Shimamura, T .; Shimoda, M .; Takai, Y .; Tanaka, H .;Terawaki, Y .; Usami, T. ; Ute, K .; Yonemitsu, T ., NMR Measurements ofIdentical Polymer Samples by Round-Robin Method .3. Analysis of FrequencyDependences of C-13 Spin-Lattice Relaxation-Times and Nuclear OverhauserEnhancements. Polymer Journal, 1992, 24,(10), 1155-1164.



1993
  1. Nicholson,Linda. K., Asakura, Tetsuo., Demura, Makoto. and Cross, Thimosy. A., A Methodfor Studying the Structure of Uniaxially Aligned Biopolymers Using Solid-StateN-15-Nmr-Application to Bombyx-Mori Silk Fibroin Fibers, Biopolymers, 33-5,847-861, 1993.
  2. Asakura,Tetsuo., Sakaguchi, Ryuji., Demura, Makoto., Manabe, Takuro., Uyama, Atsuo.,Ogawa, Katsuaki. and Osanai, Minoru., Invitro Production of Bombyx-MoriSilk Fibroin by Organ-Culture of the Posterior Silk Glands - Isotope Labelingand Fluorination of the Silk Fibroin, Biotechnol. Bioeng., 41-2,245-252, 1993.
  3. Williamson,Michael P. and Asakura, Tetsuo., Empirical Comparisons of Models forChemical-Shift Calculation in Proteins, J Magn Reson B, 101-1, 63-71,1993.
  4. Asakura,Tetsuo., Yeo, Joo-Hong., Demura, Makoto., Itoh, Takuro., Fujito, Teruaki.,Imanari, Mamoru., Nicholson, Linda. K. and Cross, Timothy. A.,Structural-Analysis of Uniaxially Aligned Polymers Using Solid-State 15NNmr, Macromolecules, 26-24, 6660-6663, 1993.
  5. Kanezaki,Takashi., Kume, Kazuo., Sato, Kazuo. and Asakura, Tetsuo., 13Cn.m.r. determination of the isotacticity of the propylene homopolymer part inethylene-propylene block copolymers, Polymer, 34-14, 3129-3131, 1993.



1994
  1. Asakura,Tetsuo. and David, L. Kaplan., Silk Production and Processing, in "Encyclopediaof Agricultural Science", Ed. byC.J.Arutzen, Academic Press, 26, 1405-1408, 1994.
  2. Asakura,Tetsuo., Demura, Makoto, Uyama, Atsuo., Ogawa, Katsuaki., Ogawa, Keiichi.,Nicholson, Linda. K. and Timothy, A. Cross, NMR Characterization of SilkProteins, ACS Symposium Series; Silks; Biology, Structure, Properties, Gentics,ACSBooksDepartment,in Chapter 13, 148-154, 1994.
  3. Asakura,Tetsuo, Demura, Makoto and Hayashi, Tetsuo, 13C NMR Assignments of Polyolefinesand Olefine Copolymers Based on the 13C NMR Chemical ShiftCalculations and 2D INADEQUATE NMR, Annu. Rep. NMR Spectrosc, 29,325-404, 1994.
  4. Ono,Atsusi., Miyauchi, Seizi., Demura, Makoto., Asakura, Tetsuo. and Kamo, Naoki.,Activation-Energy for Permeation of Phosphonium Cations throughPhospholipid-Bilayer Membrane, Biochemistry (Mosc).33-14, 4312-4318,1994.
  5. Asakura,Tetsuo., Demura, Makoto., Hiraishi, Yoshiaki., Ogawa, Katsuaki. and Uyama,Atsuo., Determination of the Structure of [1-13C]Glycine-[15N]AlanineDouble-Labeled Bombyx-Mori Silk Fibroin Fibers Using Solid-State 15NNmr, Chem. Lett, 23-12, 2249-2252, 1994.
  6. Demura,Makoto. and Asakura, Tetsuo., Structural Characterization of Samia cynthisricini Silk Fibroin as Biomaterial, Int. J. wild silkmoth & silk, 1-2,139-141, 1994.
  7. Demura,Makoto. and Asakura, Tetsuo., Structural characterization of Samia cynthiaricini silk fibroin as a biomaterial, Int. J. wild Silkmoth & Silk, 1-2,139-141, 1994.
  8. Yeo,Joo-Hong., Asakura, Tetsuo. and Shimazaki, Hisashi., Structural-Analyses ofPoly(M-Xylene-Alpha,Alpha'-Diyladipamideand Nylon-66 by N-15 and Solid-State Nmr, Macromol. Chem. Phys, 195-4,1423-1431, 1994.
  9. Kanezaki,Takashi., Kijima, Masato., Kume, Kazuo., Sato, Kazuo. and Asakura, Tetsuo., 13CNmr Sequence-Analysis of Ethylene-α-MethylstyreneCopolymers, Polymer, 35-12, 2523-2527, 1994.
  10. Asakura,Tetsuo., Yeo, Joo-Hong. and Ando, Isao., Structure of Polyamide Fibers in theNoncrystalline Domain Studied by N-15 Solid-State Nmr, Polym. J, 26-2,229-233, 1994.
  11. Asakura,Tetsuo., Aoki, Akira., Demura, Makoto., James, M. Joers., Richard, C. Rosanske.and Terry, Gullion., Structure of Bombyx-Mori Silk Fibroin Studied byRedor Nmr-Spectroscopy, Polym. J, 26-12, 1405-1408, 1994.
  12. Asakura,Tetsuo., Demura, Makoto., Uyama, A., Ogawa, K., Komatsu, K., Nicholson, L. K.and Cross, T. A., Nmr Characterization of Silk Proteins, Silk Polymers,544, 148-154, 1994.
  13. Yeo,Joo-Hong., Demura, Makoto., Asakura, Tetsuo., Fujito, Teruaki., Imanari,Mamoru., Nicholson, Linda. K. and Timothy, A. Cross, Structural-Analysis ofHighly Oriented Poly(P-Phenylene Terephthalamide) by 15NSolid-State Nuclear-Magnetic-Resonance, Solid State Nucl. Magn. Reson.,3-4, 209-218, 1994.
  14. 呂奏洪 and 朝倉哲郎, 「固体15N NMRによる配向高分子の構造解析の理論」, 高分子論文集, 51-1,43-46, 1994.
  15. 呂奏洪, 出村誠, 小中沢岳仁, 朝倉哲郎, 伊藤卓郎, 藤戸輝昭 and 今成司, 「固体15N NMRによるポリアミド系繊維の構造解析」, 高分子論文集, 51-1,47-51, 1994.
  16. 菊地淳, 藤田憲一,Williamson, Michael P. and 朝倉哲郎, 「1H NMR化学シフト計算法を導入したタンパク質溶液構造解析システムの開発」, 高分子論文集, 51-6,409-413, 1994.
  17. 青木明良, 中山信彦, 林哲男 and 朝倉哲郎, 「エチレンープロピレンー1-ブテン共重合体の13C NMRスペクトルの帰属と構造解析」, 高分子論文集, 51-10,676-684, 1994.
  18. Minami,Masashi., Takatsu, Rika., Demura, Makoto. and Asakura, Tetsuo., A Study on theHydration of Bombyx mori Silk Fibroin by Nuclear Magnetic ResonanceSpectroscopy, 繊維学会誌, 50-11,498-504, 1994.
  19. □朝倉哲郎, シルクで診断を, “シルクの科学”, 日本学術会議蚕糸学研究連絡委員会編, 朝倉書店,1994, 172-177
    20. □朝倉哲郎, 呂奏洪, 固体NMRによる高配向高分子材料の構造解析−理論アプローチと構造解析への応用−, 表面, 1994, 32, 4,264-270
    2
  20. □朝倉哲郎, 繊維と固体NMR, 繊維学会誌,1994, 50, 3-4



-1995
  1. Asakura,Tetsuo., Polymers: Regio-Irregular Structure. (Encyclopediaof Nuclear Magnetic Resonance, 3722-3727), (Ed.D.M. Grant and R.K.Harris) (John Wiley &Sons, London), 1995.
  2. Nishiyama,Norihiro., Asakura, Tetsuo., Suzuki, Kazuomi., Horie, Kozo. and Nemoto,Kimiya., Effects of a Structural-Change in Collagen Upon Binding to ConditionedDentin Studied by 13C Nmr, J. Biomed. Mater. Res., 29-1,107-111, 1995.
  3. Asakura,Tetsuo., Taoka, Kazuhiro., Demura, Makoto. and Williamson, Michael P., TheRelationship between Amide Proton Chemical-Shifts and Secondary Structure inProteins, J. Biomol. NMR, 6-3, 227-236, 1995.
  4. Williamson,Michael P., Kikuchi, Jun. and Asakura, Tetsuo., Application of 1H-NmrChemical-Shifts to Measure the Quality of Protein Structures, J. Mol. Biol.,247-4, 541-546, 1995.
  5. Umemoto,Kimiko., Kikuchi, Jun., Narita, Mitsuaki., Fujita, Kenichi. and Asakura,Tetsuo., Conformations of Synthetic Model Peptides for Plasmodium-FalciparumCircumsporozoite Protein in Me2So by H-1-Nmr and Distance GeometryCalculations, Polym. J, 27-4, 347-360, 1995.
  6. □朝倉哲郎, 出村誠, 絹生産設計, 新繊維科学−ニューフロンティアへの挑戦−, 通商産業調査,1995, 475-479
  7. □朝倉哲郎, 角度依存固体NMRによるタンパク質繊維の原子座標の決定, 生物物理,1995, 35, 280-282
  8. □朝倉哲郎, 山延健, 黒子弘道, 合成高分子｢構造解析｣‘新高分子実験学5巻｢高分子の構造（1）−磁気共鳴｣’(安藤勲編), 共立出版,1995, 238-269



1996
  1. Uchiyama,Taketo., Woltering, Thomas J., Wong, Weichyun, Lin, Chun-Cheng, Kajimoto,Tetsuya., Takebayashi, Maki., Wéitz-Schmidt,Gabriel, Asakura, Tetsuo., Noda, Masatoshi. and Wong, Chi-Huey, Design andsynthesis of C-linked fucosides as inhibitors of E-selectin, Bioorg. Med.Chem., 4-7, 1149-1165, 1996.
  2. Matsuzaki,Kei., Uryu, Toshiyuki. and Asakura, Tetsuo., NMR spectroscopy andstereoregularity of polymers, Japan Scientific Societies Press, Tokyo,275, 1996.
  3. Nishiyama,Norihiro., Suzuki, Kazuomi., Asakura, Tetsuo., Nakai, Hiroyuki., Yasuda,Seijiro. and Nemoto, Kimiya., The effects of pH of N-methacryloyl glycineprimer on bond strength to acid-etched dentin, J. Biomed. Mater. Res., 31-3,379-384, 1996.
  4. Asakura,Tetsuo., Iwadate, Mitsuo., Date, Takeshi., Demura, Makoto. and Nokihara,Kiyoshi., Refinement of the Solution Structure of Neurokinin A (4-10)on the Basic of 1H NMR Chemical Shift Calculations, Peptidechemistry, 1996, 345-348, 1996.
  5. Asakura,Tetsuo., Konakazawa, Takehito., Demura, Makoto., Ito, Takuro. and Maruhashi,Yoshitsugu., Structural analysis of uniaxially oriented C-13-labelled poly(ethyleneterephthalate) films studied with solid-state C-13 nuclear magnetic resonancespectroscopy, Polymer, 37-10, 1965-1973, 1996.
  6. Asakura,Tetsuo., Aoki, Akira., Date, Takeshi., Demura, Makoto. and Asanuma, Tadashi.,High resolution solid state 13C NMR spectroscopy of polypropylenewith very high syndiospecificity, Polym. J, 28-1, 24-29, 1996.



1997
  1. Asakura,Tetsuo., Demura, Makoto. and Nishikawa, Naoki., Structural Analysis of OrientedPolymers by Solid-state NMR, Annu. Rep. NMR Spectrosc, 34, 301-346,1997.
  2. Asakura,Tetsuo., Demura, Makoto., Date, Takeshi., Miyashita, Naoshi. and Williamson,Michael P., NMR study of silk I structure of Bombyx mori silk fibroinwith 15N- and 13C-NMR chemical shift contour plots,Biopolymers, 41-2, 193-203, 1997.
  3. Asakura,Tetsuo., Minami, Masashi., Shimada, Reiko., Demura, Makoto., Osanai, Minoru.,Fujito, Teruaki., Imanari, Mamoru. and Ulrich, Anne. S., 2H-Labelingof silk fibroin fibers and their structural characterization by solid-state 2HNMR, Macromolecules, 30-8, 2429-2435, 1997.
  4. Williamson,Michael P. and Asakura, Tetsuo., Protein Chemical Shifts, Methods in MolecularBiology, Protein NMR Techniques Edited by D. G. Reid Humana PressInc.,Totowa, NJ, 60, 53-69, 1997.
  5. □Asakura, T.; Iwadate, M.; Date, T.; Demura, M.;Nokihara,K., Refinement of the Solution Structure of Neurokinin A (4-10) on theBasis of 1H NMR Chemical Shift Calculations. Peptide Chemistry, 1996 1997,345-348.
  6. □Asakura, T.; Demura, M.; Naoki, N., StructuralAnalysis of Oriented Polymers by Solid State NMR, (Annual Reports on NMRSpectroscopy) (Ed. G.A. Webb) (ACADEMIC PRESS, London), 1997, 34, 301-346.
  7. □Asakura, T., NMR study on Fiber Structure. SEN-IGAKKAISHI, 1997, 53, 300-304.



1998
  1. Iwadate,Mitsuo., Asakura, Tetsuo. and Williamson, Michael P., The structure of themelittin tetramer at different temperatures - An NOE-based calculation withchemical shift refinement, Eur. J. Biochem., 257-2, 479-487, 1998.
  2. Nishiyama,Norihiro., Asakura, Tetsuo., Suzuki, Kazuomi., Sato, Tatsusako. and Nemoto, Kimiya.,Adhesion mechanisms of resin to etched dentin primed with N-methacryloylglycine studied by C-13-NMR, J. Biomed. Mater. Res., 40-3, 458-463,1998.
  3. Asakura,Tetsuo., Demura, Makoto., Yamazaki, Y. and Ogawa, K., Structure of uniaxiallyaligned C-13 labeled silk fibroin fibers with solid state C-13-NMR, J. Mol.Struc, 441-2-3, 155-163, 1998.
  4. Demura,Makoto., Yamazaki, Yasunobu., Asakura, Tetsuo. and Ogawa, Katsuaki., Structureof uniaxially aligned 13C labeled silk fibroin fibers with solidstate 13C-NMR, J. Mol. Struc, 441-2–3,155-163, 1998.
  5. Asakura,Tetsuo., Yamazaki, Yasunobu., Seng, Koo Wey and Demura, Makoto., Determinationof the mutual orientation of the 15N and 13C NMR chemicalshift tensors of 13C-15N double labeled model peptidesfor silk fibroin from the dipolar-coupled powder patterns, J. Mol. Struc,446-3, 179-190, 1998.
  6. Demura,Makoto., Minami, Masashi., Asakura, Tetsuo. and Cross, T. A., Structure ofBombyx mori Silk Fibroin Based on Solid-State NMR Orientational Constraintsand Fiber Diffraction Unit Cell Parameters, J. Am. Chem. Soc., 120-6,1300-1308, 1998.
  7. Nishikawa,Naoki., Tanizawa, Yoshiaki., Tanaka, Shoichi., Horiguchi, Yasunobu., Matsuno,Hitomi. and Asakura, Tetsuo., Carbon-13 n.m.r. studies of keratin intermediatefilament of human hair, Polymer, 39-4, 1001-1004, 1998.
  8. Nishikawa,Naoki., Tanizawa, Yoshiaki., Tanaka, Shoichi., Horiguchi, Yasunobu. andAsakura, Tetsuo., Structural change of keratin protein in human hair bypermanent waving treatment, Polymer, 39-16, 3835-3840, 1998.
  9. Nishikawa,Naoki., Tanizawa, Yoshiaki., Tanaka, Shoichi., Horiguchi, Yasunobu., Matsuno,Hitomi. and Asakura, Tetsuo., pH dependence of the coiled-coil structure ofkeratin intermediate filament in human hair by 13C NMR spectroscopyand the mechanism of its disruption, Polym. J, 30-2, 125-132, 1998.
  10. Asakura,Tetsuo. and Demura, Makoto., Oriented Fibers and Polymers in "SolidState NMR of Polymers", Studies inPhysical and Theoretical Chemistry, 84, 307-326, 1998.
  11. Aoki,Akira. and Asakura, Tetsuo., Polyolefins in "SolidState NMR of Polymers", Studies inPhysical and Theoretical Chemistry, 84, 415-444, 1998.
  12. Ando,Isao. and Asakura, Tetsuo., Polyamides in "SolidState NMR of Polymers", Studies inPhysical and Theoretical Chemistry, 84, 445-468, 1998.
  13. Asakura,Tetsuo. and Ito, Takuro., Poly (ethyleneterephthalate) in "Solid State NMR of Polymers", Studiesin Physical and Theoretical Chemistry, 84, 491-507, 1998.
  14. Asakura,Tetsuo., Demura, Makoto., Nishikawa, Naoki. and Yoshimizu, Hiroaki., FibrousProteins in "SolidState NMR of Polymers", Studies inPhysical and Theoretical Chemistry, 84, 853-890, 1998.



1999
  1. Asakura,Tetsuo., Polymers: Regio-Irregular Structure, 3722-3727, 1999.
  2. Kikuchi,Jun., Mitsui, Yuki., Asakura, Tetsuo., Hasuda, Katsumi., Araki, Hiromitsu. andOwaku, Kouji., Spectroscopic investigation of tertiary fold of staphylococcalprotein A to explore its engineering application, Biomaterials, 20-7,647-654, 1999.
  3. Ueki,Masaaki., Ikeo, Takayoshi., Iwadate, Mitsuo., Asakura, Tetsuo., Williamson.,Michael P. and Slaninova, Jirina., Solid phase synthesis and biologicalactivities of [Arg8]-vasopressin methylenedithioether, Bioorg.Med. Chem. Lett., 9-13, 1767-1772, 1999.
  4. Kikuchi,Jun., Asakura, Tetsuo., Loach, Paul A., Parkes-Loach, Pamela S., Shimada,Keizo., Hunter, C. Neil, Conroy, Matthew J. and Williamson, Michael P., Alight-harvesting antenna protein retains its folded conformation in the absenceof protein-lipid and protein-pigment interactions, Biopolymers, 49-5,361-372, 1999.
  5. Nakazawa,Yasumoto., Nakai, Toshimoto., Kameda, Tsunenori. and Asakura, Tetsuo., A 13CNMR study on the structural change of silk fibroin from Samia cynthia ricini,Chemical Physics Letters, 311-5, 362-366, 1999.
  6. Higuchi,Akon., Uchiyama, Shigeru., Demura, Makoto., Asakura, Tetsuo., Cho, Chong-Su.,Akaike, Toshihiro., Takarada, Hirokazu. and Hara, Mariko., Enhanced CEAproduction associated with aspirin in a culture of CW-2 cells on some polymericfilms, Cytotechnology, 31-3, 233-242, 1999.
  7. Hori,Yumiko., Demura, Makoto., Niidome, Takuro., Aoyagi, Haruhiko. and Asakura,Tetsuo., Orientational behavior of phospholipid membranes with mastoparanstudied by 31P solid state NMR, FEBS Lett., 455-3, 228-232,1999.
  8. Asakura,Tetsuo, Iwadate, Mitsuo, Demura, Makoto and Williamson, Michael P., Structuralanalysis of silk with 13C NMR chemical shift contour plots,Int.J._Biol. Macromol., 24-2–3, 167-171,1999.
  9. Asakura,Tetsuo. and Kikuchi, Jun., Use of 13C conformation-dependentchemical shifts to elucidate the local structure of a large protein withhomologous domains in solution and solid state, J. Biochem. Biophys. Methods,38-3, 203-208, 1999.
  10. Kikuchi,Jun. and Asakura, Tetsuo., Use of 13C conformation-dependentchemical shifts to elucidate the local structure of a large protein withhomologous domains in solution and solid state, J. Biochem. Biophys. Methods,38-3, 203-208, 1999.
  11. Williamson,Michael P., Iwadate, Mitsuo. and Asakura, Tetsuo., Ca andCbcarbon-13 chemical shifts in proteins from an empirical database, J. Biomol.NMR, 13-3, 199-211, 1999.
  12. Asakura,Tetsuo. and Demura, Makoto., Structure and dynamics of silk fibroin studiedwith 13C, 15N and 2H solid state NMR,Macromol. Symp, 143, 1-10, 1999.
  13. Asakura,Tetsuo., Ito, Takuro., Okudaira, Mami. and Kameda, Tsunenori., Structure ofalanine and glycine residues of Samia cynthia ricini silk fibers studiedwith solid-state 15N and 13C NMR, Macromolecules,32-15, 4940-4946, 1999.
  14. Kameda,Tsunenori., Ohkawa, Yohei., Yoshizawa, Keiko., Naito, Junko., Ulrich, Anne. S.and Asakura, Tetsuo., Hydrogen-Bonding Structure of Serine Side Chains inBombyx mori and Samia cynthia ricini Silk Fibroin Determined bySolid-State 2H NMR, Macromolecules, 32-21, 7166-7171, 1999.
  15. Kameda,Tsunenori., Ohkawa, Youhei., Yoshizawa, Keiko., Nakano, Emi., Hiraoki,Toshifumi., Ulrich, Anne. S. and Asakura, Tetsuo., Dynamics of the TyrosineSide Chain in Bombyx mori and Samia cynthia ricini Silk FibroinStudied by Solid State 2H NMR, Macromolecules, 32-25,8491-8495, 1999.
  16. Nishikawa,Noaki., Horiguchi, Yasunobu., Asakura, Tetsuo. and Ando, Isao., Carbon-13solid-state n.m.r. study of 13C-enriched human hair keratin,Polymer, 40-8, 2139-2144, 1999.