Original Paper



2000
  1. Higuchi,Akon., Yoshida, Makoto., Ohno, Takeshi., Asakura, Tetsuo. and Hara, Mariko.,Production of interferon-beta in a culture of fibroblast cells on somepolymeric films, Cytotechnology, 34-1-2, 165-173, 2000.
  2. Iwadate,Mitsuo., Nagao, Eriko., Williamson, Michael P., Ueki, Masaaki. and Asakura,Tetsuo., Structure determination of [Arg8]vasopressin methylenedithioether indimethylsulfoxide using NMR, Eur. J. Biochem., 267-14, 4504-4510, 2000.
  3. Osanai,Minoru., Okudaira, Mami., Naito, Junko., Demura, Makoto. and Asakura, Tetsuo.,Biosynthesis of L-alanine, a major amino acid of fibroin in Samia cynthiaricini, Insect Biochem. Mol. Biol., 30-3, 225-232, 2000.
  4. Kikuchi,Jun., Asakura, Tetsuo., Hasuda, Katsumi., Ito, Takuro., Ohwaku, Kouji., Araki,Hiromitsu. and Williamson, Michael P., An advantage for use of isotope labelingand NMR chemical shifts to analyze the structure of four homologous IgG-bindingdomains of staphylococcal protein A, J. Biochem. Biophys. Methods, 42-1-2,35-47, 2000.
  5. Hara, Mariko., Asakura, Tetsuo., Cho, Chong-Su., Akaike, Toshihiro. and Higuchi,Akon., Morphologies of PC12 Cells Cultured on Some Polymeric Films-Relationship between Cell Growth and Surface Physical Properties-, J. Chem.Soc. Jap., Chem. Indus. Chem, 4, 257-265, 2000.
  6. Beek,J. D. van, Beaulieu, L., Schäfer, H., Demura,Makoto., Asakura, Tetsuo. and Meier, B. H., Solid-state NMR determination ofthe secondary structure of Samia cynthia ricini silk, Nature, 405,1077-1079, 2000.
  7. Kikuchi,Jun., Williamson, Michael P., Shimada, Keizo. and Asakura, Tetsuo., Structureand dynamics of photosynthetic membrane-bound proteins in RhodobacterSphaeroides, studied with solid-state NMR spectroscopy, Photosynth Res,63-3, 259-267, 2000.
  8. Ito,Takuro., Maruhashi, Yoshitsugu., Demura, Makoto. and Asakura, Tetsuo.,Carbon-13 solid state NMR study on uniaxially oriented poly(L-lacticacid) films, Polymer, 41-3, 859-866, 2000.
  9. 朝倉哲郎, 研究室紹介(東京農工大学工学部生命工学科朝倉研究室-自然に学ぶ-), 日本接着学会誌, 36, 293-294, 2000.
  10. 増田裕美, 姚菊明, 亀田恒徳, 勝野盛夫, 石坂弘子, 朝倉哲郎, 臭化リチウム/エタノール/水混合系での再生家蚕絹フィブロイン繊維の作成とキャラクタリゼーション, 製糸絹研究会誌, 9, 35-40, 2000.
  11. 朝倉哲郎, 絹の繊維化前の構造と巧みな繊維化のメカニズム 野蚕, 40, 3-5, 2000.
  12. Nishiyama, N., Asakura, Tetsuo., Suzuki, K., Komatsu, K., Nemoto, K., Bond strength of resin to acid-etched dentin studied by C-13 NMR:Interaction between N-methacryloyl-omega-amino acid primer and dentinalcollagen. Journal of Dental Research, 79-3, 806-811, 2000.



2001
  1. Asakura,Tetsuo., Yamane, Tsutomu., Nakazawa, Yasumoto., Kameda, Tsunenori. and Ando,Kazuto., Structure of Bombyx mori silk fibroin before spinning in solidstate studied with wide angle x-ray scattering and 13Ccross-polarization/magic angle spinning NMR, Biopolymers, 58-5, 521-525, 2001.
  2. Hori,Yumiko., Demura, Makoto., Iwadate, Mitsuo., Ulrich, Anne. S., Niidome, Takuro.,Aoyagi, Haruhiko. and Asakura, Tetsuo., Interaction of mastoparan withmembranes studied by 1H NMR spectroscopy in detergent micelles andby solid-state 2H NMR and 15N NMR spectroscopy inoriented lipid bilayers, Eur. J. Biochem., 268-2, 302-309, 2001.
  3. Nishiyama,Norihiro., Suzuki, Kazumi., Asakura, Tetsuo., Komatsu, Kohei. and Nemoto,Kimiya., Adhesion of N-methacryloyl-ω-amino acidprimers to collagen analyzed by 13C NMR, J. Dent. Res, 80-3,855-859, 2001.
  4. Ito,Takuro., Yamaguchi, Yuji., Watanabe, Hiroto. and Asakura, Tetsuo., Structuralanalysis of oriented poly(ε-caprolactone)including CaCO3 particles with 13C solid-state NMR, J.Appl. Polym. Sci, 80-12, 2376-2382, 2001.
  5. Iwadate,Mitsuo., Asakura, Tetsuo., Dubovskii, P. V., Yamada, Hiroaki., Akasaka,Kazuyuki. and Williamson, Michael P., Pressure-dependent changes in thestructure of the melittin alpha-helix determined by NMR, J. Biomol. NMR,19-2, 115-124, 2001.
  6. Asakura,Tetsuo., Ashida, Jun., Yamane, Tsutomu., Kameda, Tsunenori, Nakazawa,Yasumoto., Ohgo, Kosuke. and Komatsu, Kohei., A repeated beta-turn structure inpoly(Ala-Gly)as a model for silk I of Bombyx mori silk fibroin studied withtwo-dimensional spin-diffusion NMR under off magic angle spinning androtational echo double resonance, J. Mol. Biol., 306-2, 291-305, 2001.
  7. Shiroishi,Hidenobu., Sadohara, Hitomi., Asakura, Tetsuo. and Kaneko, Masao.,Characteristics of photoluminescence from ruthenium polypyridyl complexesincorporated into silk, J. Photochem. Photobiol. A, 143-2-3, 147-151,2001.
  8. Monti,Patrizia., Taddei, Paola., Freddi, Giuliano., Asakura, Tetsuo. and Tsukada,Masuhiro., Raman spectroscopic characterization of Bombyx mori silkfibroin: Raman spectrum of Silk I, J. Raman Spectrosc, 32-2, 103-107,2001.
  9. Zhao,Chenhua. and Asakura, Tetsuo., Structure of Silk studied with NMR, Prog.Nucl. Magn. Reson. Spectrosc, 39-4, 301-352, 2001.
  10. 朝倉哲郎, 絹と繊維化前の構造と巧みな繊維化のメカニズム, ブレインテクノニュース, 83, 12-14, 2001.
  11. 小山内実, 奥平真実, カイコガおよびエリサンガの非必須アミノ酸の生合成と尿素回路, 蛋白質 核酸 酵素, 46, 6,733-739, 2001.
  12. Asakura, Tetsuo., Ashida, J., NMR. 高分子, 50-8, 549-552, 2001.



2002
  1. Kameda,Tsunenori. and Asakura, Tetsuo., Dynamics of silk fibroin studied with NMR spectroscopy,Annu. Rep. NMR Spectrosc, 46, 101-149, 2002.
  2. Asakura,Tetsuo., Sugino, Rena., Yao, Juming., Takashima, Hidehiko. and Raghuvansh, Kishore.,Comparative structure analysis of tyrosine and valine residues in unprocessed silkfibroin (silk Ⅰ) andin the processed silk fiber (silk Ⅱ) fromBombyx mori using solid-state 13C, 15N, and 2HNMR, Biochemistry (Mosc).41-13, 4415-4424, 2002.
  3. Kameda,Tsunenori, Nakazawa, Yasumoto., Kazuhara, Junko., Yamane, Tsutomu. and Asakura,Tetsuo., Determination of intermolecular distance for a model peptide of Bombyxmori silk fibroin, GAGAG, with rotational echo double resonance, Biopolymers,64-2, 80-85, 2002.
  4. Higuchi,Akon., Takanashi, Yasunari., Ohno, Takeshi., Asakura, Tetsuo., Cho, Chong-Su., Akaike,Toshihiro. and Hara, Mariko., Production of interferon-beta by fibroblast cellson membranes prepared by extracellular matrix proteins, Cytotechnology, 39-3,131-137, 2002.
  5. Nakazawa,Yasumoto. and Asakura, Tetsuo., Heterogeneous exchange behavior of Samia cynthiaricini silk fibroin during helix-coil transition studied with 13CNMR, FEBS Lett., 529-2-3, 188-192, 2002.
  6. Demura,Makoto., Noda, Masatoshi, Kajimoto, Tetsuya., Uchiyama, Taketo., Umemoto, Kimiko.,Wong, Chi-Huey and Asakura, Tetsuo., Solution structure of sialyl Lewis X mimicsstudied by two-dimensional NMR, J. Mol. Struc, 602, 215-222, 2002.
  7. Asakura,Tetsuo., Yao, Juming., Yamane, Tsutomu., Umemura, Kosuke. and Ulrich, Anne. S.,Heterogeneous structure of silk fibers from Bombyx mori resolved by 13Csolid-state NMR spectroscopy, J. Am. Chem. Soc., 124-30, 8794-8795, 2002.
  8. Yao,Juming., Masuda, Hiromi., Zhao, Chenhua. and Asakura, Tetsuo., Artificial spinningand characterization of silk fiber from Bombyx mori silk fibroin in hexafluoroacetonehydrate, Macromolecules, 35-1, 6-9, 2002.
  9. Nakazawa, Yasumoto. and Asakura, Tetsuo., High-resolution 13C CP/MAS NMR studyon structure and structural transition of Antheraea pernyi silk fibroin containingpoly(L-alanine)and gly-rich regions, Macromolecules, 35-6, 2393-2400, 2002.
  10. Yamane, Tsutomu., Umemura, Kosuke. and Asakura, Tetsuo., The structural characteristicsof Bombyx mori silk fibroin before spinning as studied with molecular dynamicssimulation, Macromolecules, 35-23, 8831-8838, 2002.
  11. Kameda,Tsunenori, Kobayashi, Masatoshi., Yao, Juming. and Asakura, Tetsuo., Change in thestructure of poly(tetramethylene succinate) under tensile stressmonitored with solid state 13C NMR, Polymer, 43-4, 1447-1451,2002.
  12. Asakura,Tetsuo., Kato, Hidetoshi., Yao, Juming., Raghuvansh, Kishore. and Shirai, Makoto.,Design, expression, and structural characterization of hybrid proteins of Samiacynthia ricini and Bombyx mori silk fibroins, Polym. J, 34-12,936-943, 2002.
  13. Asakura,Tetsuo., Sugino, Rena., Okumura, Tatsushi. and Nakazawa, Yasumoto., The role ofirregular unit, GAAS, on the secondary structure of Bombyx mori silk fibroinstudied with 13C CP/MAS NMR and wide-angle X-ray scattering, ProteinSci., 11-8, 1873-1877, 2002.
  14. Asakura,Tetsuo. and Yao, Juming., 13C CP/MAS NMR study on structural heterogeneityin Bombyx mori silk fiber and their generation by stretching, ProteinSci., 11-11, 2706-2713, 2002.
  15. 山根努, 園山正史, 朝倉哲郎 and 古川行夫, 「Silk Ⅰ型家蚕フィブロインモデル化合物(Ala-Gly)15のラマンスペクトルと繰り返しβターンタイプⅡ型構造モデルに基づく理論的計算」, 繊維学会誌, 58-9,327-331, 2002.
  16. 共著, 高分子辞典(第3版), 朝倉書店, 2002.
  17. 朝倉哲郎, 新しい絹様材料の開発-分子設計, 生産, そして繊維化への挑戦, 未来材料エヌ・ティー・セス, 2, 31-36, 2002.
  18. 朝倉哲郎, 大学化学教育の改革(その9)教育褒賞制度(BT:ベストティーチャー制度), 化学と教育, 50, 476-477, 2002.
  19. 朝倉哲郎, 最新の固体NMRの手法を用いた家蚕絹繊維化前後の構造の決定, 高分子加工,2002, 51, 338-342
  20. Ashida, J., Ohgo, K., Asakura, Tetsuo., Determination of the torsion angles of alanine andglycine residues of Bombyx mori silk fibroin and the model peptides in the silkI and silk II forms using 2D spin diffusion solid-state NMR under off magicangle spinning., Journal of Physical Chemistry B, 106-36, 9434-9439, 2002.
  21. Matsuda, H., Asakura, Tetsuo., Miki, T., Triad sequence analysis of poly(ethylene/butyleneterephthalate) copolymer using H-1 NMR., Macromolecules, 35-12, 4664-4668, 2002.
  22. Asakura, Tetsuo., Ashida, J., Yamane, T., Structure of Bombyx mori Silk Fibroin beforeSpinning in Silkworm (Chap.6). Symposium Series No.834 NMR Spectroscopy ofPolymers in Solution and in the Solik State, Ed. H.N.Cheng and A.D.English, 2002.



2003
  1. Asakura,Tetsuo., Nitta, Koji., Yang, Mingying., Yao, Juming., Nakazawa, Yasumoto. and David,L. Kaplan., Synthesis and characterization of chimeric silkworm silk, Biomacromolecules,4-3, 815-820, 2003.
  2. Zhao,Chenhua., Yao, Juming., Masuda, Hiromi., Raghuvansh, Kishore. and Asakura, Tetsuo.,Structural characterization and artificial fiber formation of Bombyx morisilk fibroin in hexafluoro-iso-propanol solvent system, Biopolymers, 69-2,253-259, 2003.
  3. Monti,Patrizia., Taddei, Paola., Freddi, Giuliano., Ohgo, Kosuke. and Asakura, Tetsuo.,Vibrational 13C-cross-polarization/magic angle spinning NMR spectroscopicand thermal characterization of poly(alanine-glycine)as model for silk I Bombyx mori fibroin, Biopolymers, 72-5, 329-338,2003.
  4. Higuchi,Akon., Takanashi, Yasunari., Tsuzuki, Nobuya., Asakura, Tetsuo., Cho, Chong-Su.,Akaike, Toshihiro. and Hara, Mariko., Production of interferon-β by fibroblastcells on membranes prepared with RGD-containing peptides, J Biomed Mater ResA, 65A-3, 369-378, 2003.
  5. Asakura,Tetsuo. and Yao, Juming., Synthesis and structural characterization of silk-likematerials incorporated with an elastic motif, J. Biochem. (Tokyo).133-1,147-154, 2003.
  6. Ashida,Jun., Ohgo, Kosuke., Komatsu, Kohei., Kubota, Ayumi. and Asakura, Tetsuo., Determinationof the torsion angles of alanine and glycine residues of model compounds of spidersilk (AGG)10using solid-state NMR methods, J. Biomol. NMR, 25-2, 91-103, 2003.
  7. Kameda,Tsunenori., Zhao, Chenhua., Ashida, Jun. and Asakura, Tetsuo., Determination ofdistance of intra-molecular hydrogen bonding in (Ala-Gly)15with silk I form after removal of the effect of MAS frequency in REDOR experiment,J Magn Reson, 160-2, 91-96, 2003.
  8. Ashida,Jun. and Asakura, Tetsuo., An application of the XiX decoupling for solid state13C NMR with mobile samples, J Magn Reson, 165-1, 180-183, 2003.
  9. Nakazawa,Yasumoto. and Asakura, Tetsuo., Structure determination of a peptide model of therepeated helical domain in Samia cynthia ricini silk fibroin before spinningby a combination of advanced solid-state NMR methods, J. Am. Chem. Soc.,125-24, 7230-7237, 2003.
  10. Terry,Gullion., Raghuvansh, Kishore. and Asakura, Tetsuo., Determining dihedral anglesand local structure in silk peptide by 13C 2H REDOR, J.Am. Chem. Soc., 125-25, 7510-7511, 2003.
  11. Matsuda,Hironori., Asakura, Tetsuo. and Nakagawa, Yasuo., Sequence analysis of Technora(copolyamideof terephthaloyl chloride, p-phenylenediamine, and 3,4 '-diaminodiphenylether) using 13C NMR, Macromolecules, 36-16, 6160-6165, 2003.
  12. Asakura,Tetsuo., Yamane, Tsutomu., Umemura, Kosuke. and Nakazawa, Yasumoto., Molecular dynamicssimulation of conformational change of poly(Ala-Gly)from silk I to silk II in relation to fiber formation mechanism of Bombyx morisilk fibroin, Macromolecules, 36-18, 6766-6772, 2003.
  13. Ohgo,Kosuke., Zhao, Chenhua., Kobayashi, Mitsuhiro. and Asakura, Tetsuo., Preparationof non-woven nanofibers of Bombyx mori silk, Samia cynthia ricini silkand recombinant hybrid silk with electrospinning method, Polymer, 44-3, 841-846,2003.
  14. Matsuda,Hironori., Nagasaka, Bunsow. and Asakura, Tetsuo., Sequence analysis of poly (ethylene/1,4-cyclohexanedimethyleneterephthalate) copolymer using 1H and 13C NMR, Polymer,44-16, 4681-4687, 2003.
  15. Kameda,Tsunenori. and Asakura, Tetsuo., Structure and dynamics in the amorphous regionof natural rubber observed under uniaxial deformation monitored with solid-state13C NMR, Polymer, 44-24, 7539-7544, 2003.
  16. Asakura,Tetsuo., Ashida, Jun. and Ohgo, Kosuke., Conformational characterization of (Val-Pro-Gly-Val-Gly)6with 13C solid state NMR, Polym. J, 35-3, 293-296, 2003.
  17. Matsuda,Hironori., Nagasaka, Bunsow. and Asakura, Tetsuo., Sequence analysis of polyarylate(U-Polymer)and its polyestercarbonate using 1H and 13C NMR, Polym.J, 35-9, 740-747, 2003.
  18. Asakura,Tetsuo., Nakazawa, Yasumoto., Bamba, Mie. and Nishio, Satoko., Tightly winding structureof sequential model peptide for repeated helical region in Samia cynthia ricinisilk fibroin studied with solid-state NMR, Protein Sci., 12-4, 666-671, 2003.
  19. 松田裕生, 山崎静夫 and 朝倉哲郎, 「全芳香族ポリアミドのN-メチル-2-ピロリドン中での1H NMR構造解析」, 高分子論文集, 60-4, 186-191, 2003.
  20. 川口謙, 木村一雄 and 朝倉哲郎, 「バイセルに結合したペプチドの高分解能1H NMR観測」, 高分子論文集, 60-4, 199-202, 2003.
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  21. 朝倉哲郎, 固体NMRによる絹の分子構造解明と新しい絹様材料の開発, 生物物理, 43-6, 281-286, 2003.
  22. 朝倉哲郎, 第5講 遺伝子組み換えで大腸菌から新しい絹を作る, 生体内の高分子, 91-108, 2003.
  23. Asakura, Tetsuo., Ashida, J., Yamane, T., Structure ofBombyx mori silk fibroin before spinning in silkworm., NMR SPECTROSCOPY OFPOLYMERS IN SOLUTION AND IN THE SOLID STATE, ACS SYMPOSIUM SERIES, 834, 71-82, 2003.



2004
  1. Yao,Juming., Nakazawa, Yasumoto. and Asakura, Tetsuo., Structures of Bombyx moriand Samia cynthia ricini silk fibroins studied with solid-state NMR,Biomacromolecules, 5-3, 680-688, 2004.
  2. Ohgo,Kosuke., Kurano, Tracie L., Kumashiro, Kristin K. and Asakura, Tetsuo.,Structure of the model peptides of Bombyx mori silk-elastin like proteinstudied with solid state NMR, Biomacromolecules, 5-3, 744-750, 2004.
  3. Asakura,Tetsuo., Yao, Juming., Ohgo, Kosuke., Sugino, Rena. and Raghuvansh, Kishore,Structural analysis of Bombyx mori silk fibroin peptides with formicacid treatment using high-resolution solid-state 13C NMRspectroscopy, Biomacromolecules, 5-5, 1763-1769, 2004.
  4. Rousseau,Marie-Eve., Beaulieu, Lilyane., Lefèvre, Thierry.,Paradis, Joanie., Asakura, Tetsuo. and Pézolet,Michel., Study of protein conformation and orientation in silkworm and spidersilk fibers using Raman microspectroscopy, Biomacromolecules, 5-6,2247-2257, 2004.
  5. Asakura,Tetsuo., Tanaka, Chikako., Yang, Mingying., Yao, Juming. and Kurokawa, Masato.,Production and characterization of a silk-like hybrid protein, based on thepolyalanine region of Samia cynthia ricini silk fibroin and a celladhesive region derived from fibronectin, Biomaterials, 25-4, 617-624,2004.
  6. Taddei,Paola., Asakura, Tetsuo., Yao, Juming. and Monti, Patrizia., Raman study ofpoly(alanine-glycine)-basedpeptides containing tyrosine, valine, and serine as model for thesemicrystalline domains of Bombyx mori silk fibroin, Biopolymers,75-4, 314-324, 2004.
  7. Yao,Juming., Asakura, Tetsuo. and Yanagisawa, Satoshi., Design, expression andcharacterization of collagen-like proteins based on the cell adhesive andcrosslinking sequences derived from native collagens, J. Biochem. (Tokyo).136-5,643-649, 2004.
  8. Matsuda,Hironori. and Asakura, Tetsuo., Longer range sequence analysis offour-component copolyester using NMR, Macromolecules, 37-6, 2163-2170,2004.
  9. Yang,Mingying., Yao, Juming., Sonoyama, Masashi. and Asakura, Tetsuo., Spectroscopiccharacterization of heterogeneous structure of Samia cynthia ricini silkfibroin induced by stretching and molecular dynamics simulation,Macromolecules, 37-9, 3497-3504, 2004.
  10. Matsuda,Hironori., Asakura, Tetsuo., Nagasaka, Bunsow. and Sato, Kazuhiko.,Relationship between Sequence Distribution and Thermal Properties of theTransesterification Product between Poly(ethyleneterephthalate) and Poly(butyleneterephthalate), Macromolecules, 37-12, 4651-4657, 2004.
  11. Asakura,Tetsuo., Suita, Kohei., Kameda, Tsunenori., Afonin, Sergii. and Ulrich, Anne.S., Structural role of tyrosine in Bombyx mori silk fibroin, studied bysolid-state NMR and molecular mechanics on a model peptide prepared as silk Iand II,Magn Reson Chem, 42-2, 258-266, 2004.
  12. Nishiyama,Toshihiro., Kajimoto, Tetsuya., Tanaka, Toru., Ozawa, Machiko., Asakura,Tetsuo., Miura, Tsuyoshi., Tsuji, Shuichi., Kasuya, Maria Carmelita. andHatanaka, Kenichi., Synthesis of Peptide Mimetics of CMP-Sialic Acid as theInhibitors of Sialyl Transferase, Peptide science 2003, 2003, 215-218,2004.
  13. Asakura, Tetsuo., Yang, Mingying. and Kawase, Taiji., Structure of characteristicsequences in Nephila clavipes dragline silk (MaSp1)studied with 13C solid state NMR, Polym. J, 36-12, 999-1003,2004.
  14. 亀田恒徳, 朝倉哲郎, 張力下における天然ゴムの構造と運動性に関する固体13CNMRを用いた研究, 高分子加工3月号, 53, 6-11, 2004.
  15. 朝倉哲郎, 「NMR」 第5版 3,2,2 核磁気共鳴スペクトル, 実験化学講座, 日本化学会(編), 丸善, 26, 271-276, 2004.
  16. 大郷耕輔, 朝倉哲郎, 「エレクトロスピニング法」機能性不織布の新展開 (監修)日向明, ㈱シーエムシー出版, 84-97, 2004.
  17. 朝倉哲郎, 「新しい絹をつくる -固体NMRで絹の構造を解き明かす-」, 現代化学6月号, 399, 24-31, 2004.
  18. 朝倉哲郎, 1.絹 第3版「繊維便覧」, 繊維学会編, 丸善, 149-152, 2004.
  19. 朝倉哲郎, 「高分子辞典」, 2004.
  20. 朝倉哲郎, 「NMRを用いた家蚕絹繊維化前の構造」, FIBER繊維学会誌, 60-11, 543-546, 2004.
  21. 朝倉哲郎, 「週刊ナノテク」, 産業タイムス社, 1187, 6-7, 2004.
  22. Asakura, Tetsuo., Nakazawa, Y., Structure and structural changes of the silk fibroin fromSamia cynthia ricini using nuclear magnetic resonance spectroscopy., Macromolecular Bioscience, 4-3, 175-185, 2004.
  23. Yao, J. M., Asakura, Tetsuo., `SILKS' Encyclopedia of biomaterials and biomedicalengineering. Marcel Dekker Inc. NY, 1363-1370, 2004.
  24. Yao, J. M., Ohgo, Kosuke., Sugino, R., Kishore, R., Asakura, Tetsuo., Structural analysis ofBombyx mori silk fibroin peptides with formic acid treatment usinghigh-resolution solid-state C-13 NMR spectroscopy. Biomacromolecules, 5-5, 1763-1769, 2004.



2005
  1. Asakura,Tetsuo., Ohgo, Kosuke., Ishida, Teppei., Taddei, Paola., Monti, Patrizia. andKishore, Raghuvansh., Possible implications of serine and tyrosine residues andintermolecular interactions on the appearance of silk I structure of Bombyxmori silk fibroin-derived synthetic peptides: High-resolution 13Ccross-polarization/magic-angle spinning NMR study, Biomacromolecules, 6-1,468-474, 2005.
  2. Yang,Mingying., Nakazawa, Yasumoto., Yamauchi, Kazuo., Knight, David P. and Asakura,Tetsuo., Structure of model peptides based on Nephila clavipes draglinesilk spidroin (MaSp1)studied by 13C cross polarization/magic angle spinning NMR,Biomacromolecules, 6-6, 3220-3226, 2005.
  3. Yang,Mingying. and Asakura, Tetsuo., Design, expression and solid-state NMRcharacterization of silk-like materials constructed from sequences of spidersilk, Samia cynthia ricini and Bombyx mori silk fibroins, J.Biochem. (Tokyo).137-6, 721-729, 2005.
  4. Yamauchi,Kazuo., Imada, Takuzo. and Asakura, Tetsuo., Use of microcoil probehead fordetermination of the structure of oriented silk fibers by solid-state NMR,J. Phys. Chem. B, 109-37, 17689-17692, 2005.
  5. Asakura,Tetsuo., Yang, Mingying., Kawase, Taiji. and Nakazawa, Yasumoto., 13Csolid-state NMR study of structural heterogeneity in peptides containing bothpolyalanine and repeated GGA sequences as a local structural model of Nephilaclavipes dragline silk (Spidroin 1),Macromolecules, 38-8, 3356-3363, 2005.
  6. Ohgo,Kosuke., Ashida, Jun., Kumashiro, Kristin K. and Asakura, Tetsuo., Structuraldetermination of an elastin-mimetic model peptide, (Val-Pro-Gly-Val-Gly)6,studied by 13C CP/MAS NMR chemical shifts, two-dimensional off magicangle spinning spin-diffusion NMR, rotational echo double resonance, andstatistical distribution of torsion angles from protein data bank,Macromolecules, 38-14, 6038-6047, 2005.
  7. Asakura,Tetsuo., Ohgo, Kosuke., Komatsu, Kohei., Kanenari, Masakazu. and Okuyama,Kenji., Refinement of repeated beta-turn structure for silk I conformation ofBombyx mori silk fibroin using 13C solid-state NMR and X-raydiffraction methods, Macromolecules, 38-17, 7397-7403, 2005.
  8. Ohtaki,Manabu., Kameda, Tsunenori., Asakura, Tetsuo. and Murase, Shigemitsu.,Structural characterization of drawn and annealed poly(trimethyleneterephthalate) fibers, Polym. J, 37-3, 214-220, 2005.
  9. Kawaguchi,Ken., Suita, Kohei., Suzuki, Yu., Umemoto, Kimiko., Nakazawa, Yasumoto. andAsakura, Tetsuo., Orientation of the antimicrobial peptide, cecropin A-magainin2 hybrid, in a lipid bilayer studied by 15N solid-state NMR,Polym. J, 37-3, 229-233, 2005.
  10. Asakura,Tetsuo., Nakazawa, Yasumoto., Ohnishi, Erika. and Moro, Fumika., Evidence from 13Csolid-state NMR spectroscopy for a lamella structure in an alanine-glycinecopolypeptide: A model for the crystalline domain of Bombyx mori silkfiber, Protein Sci., 14-10, 2654-2657, 2005.
  11. 大郷耕輔, 朝倉哲郎, 「絹フィブロインの構造と大腸菌による新しい絹の生産ならびに生体材料への応用」昆虫テクノロジー研究と産業利用, シーエムシー出版, 97-104, 2005.



2006
  1. Williamson,Michael P., Suzuki, Yu., Bourne, Nathan T. and Asakura, Tetsuo., Binding ofamyloid β-peptideto ganglioside micelles is dependent on histidine-13, Biochem. J., 397-3,483-490, 2006.
  2. Ha,Sung-Won., Asakura, Tetsuo. and Kishore, Raghuvansh., Distinctive influence oftwo hexafluoro solvents on the structural stabilization of Bombyx morisilk fibroin protein and its derived peptides: 13C NMR and CDstudies, Biomacromolecules, 7-1, 18-23, 2006.
  3. Asakura,Tetsuo., Hamada, Megumi., Nakazawa, Yasumoto., Ha, Sung-Won. and Knight, DavidP., Conformational study of silk-like peptides containing the calcium-bindingsequence from calbindin D9k using 13C CP/MAS NMR spectroscopy,Biomacromolecules, 7-2, 627-634, 2006.
  4. Ohgo,Kosuke., Kawase, Taiji., Ashida, Jun. and Asakura, Tetsuo., Solid-state NMRanalysis of a peptide (Gly-Pro-Gly-Gly-Ala)6-Glyderived from a flagelliform silk sequence of Nephila clavipes,Biomacromolecules, 7-4, 1210-1214, 2006.
  5. Asakura,Tetsuo., Hamada, Megumi., Ha, Sung-Won. and Knight, David P., ConformationalStudy of Silklike Peptides Modified by the Addition of the Calcium-BindingSequence from the Shell Nacreous Matrix Protein MSI60 Using 13C CP/MASNMR Spectroscopy, Biomacromolecules, 7-6, 1996-2002, 2006.
  6. Pézolet,Michel., Rousseau, Marie-Eve., Beaulieu, Lilyane., Lefèvre,Thierry., Paradis, Joanie. and Asakura, Tetsuo., Characterization by Ramanmicrospectroscopy of the strain-induced conformational transition in fibroinfibers from the silkworm Samia cynthia ricini, Biomacromolecules, 7-9,2512-2521, 2006.
  7. Ohgo,Kosuke., Niemczura, Walter P., Ashida, Jun., Okonogi, Michi., Kumashiro,Kristin K. and Asakura, Tetsuo., Heterogeneity in the conformation of valine inthe elastin mimetic (LGGVG)6 as shown bysolid-state 13C NMR spectroscopy, Biomacromolecules, 7-12,3306-3310, 2006.
  8. Yamauchi,Kazuo. and Asakura, Tetsuo., Development of microMAS NMR probehead formass-limited solid-state samples, Chem. Lett, 35-4, 426-427, 2006.
  9. Kino,Rikako., Ikoma, Toshiyuki., Monkawa, Akira., Yunoki, Shunji., Munekata,Masanobu., Tanaka, Junzo. and Asakura, Tetsuo., Deposition of bone-like apatiteon modified silk fibroin films from simulated body fluid, J. Appl. Polym.Sci, 99-5, 2822-2830, 2006.
  10. Asakura,Tetsuo., Okonogi, Michi., Nakazawa, Yasumoto. and Yamauchi, Kazuo., Structuralanalysis of alanine tripeptide with antiparallel and parallel b-sheetstructures in relation to the analysis of mixed b-sheet structuresin Samia cynthia ricini silk protein fiber using solid-state NMRspectroscopy, J. Am. Chem. Soc., 128-18, 6231-6238, 2006.
  11. Kino,Rikako., Ikoma, Toshiyuki., Yunoki, Shunji., Monkawa, Akira., Matsuda,Atsushi., Kagata, Go., Asakura, Tetsuo., Munekata, Masanobu. and Tanaka,Junzo., Biodegradation of multilayer silk fibroin and hydroxyapatite compositematerial, Key Engineering Materials, 309-311, 1169-1172, 2006.
  12. Teramoto,Hidetoshi., Kakazu, Aya. and Asakura, Tetsuo., Native structure and degradationpattern of silk sericin studied by 13C NMR spectroscopy,Macromolecules, 39-1, 6-8, 2006.
  13. Ando,Isao. and Asakura, Tetsuo., NMR Chemical Shift Map「Modern Magnetic Resonance」 Vol.1.Application in Chemistry, Springer, 33-38, 2006.
  14. Asakura,Tetsuo. and Nakazawa, Yasumoto., Structural Analysis of Silk Fibroins using NMR「ModernMagnetic Resonance」Vol.1. Application in Chemistry, Springer, 97-102, 2006.
  15. 朝倉哲郎 and 中澤靖元, 「蚕ならびにクモが生産する絹の構造の解明―主に固体NMR構造解析法を用いて」, 高分子論文集, 63-11,707-719, 2006.
  16. 朝倉哲郎, 関根素馨, 中澤靖元, 非晶構造の評価, 高分子55巻9月号, 718-721, 2006.
  17. 朝倉哲郎, 出村誠(分担), 第8章 生体高分子「基礎高分子科学」高分子学会編, 東京化学同人, 401-431, 2006.
  18. 朝倉哲郎(分担), 絹の生成過程を直接「見る」「“ファイバー"スーパーバイオミメテックス」, NTS社, 197-202, 2006.



2007
  1. Asakura,Tetsuo., Umemura, Kosuke., Nakazawa, Yasumoto., Hirose, Haruko., Higham, James.and Knight, David P., Some observations on the structure and function of thespinning apparatus in the silkworm Bombyx mori, Biomacromolecules, 8-1,175-181, 2007.
  2. Yanagisawa,Satoshi., Zhu, Zhenghua., Kobayashi, Isao., Uchino, Keiro., Tamada, Yasushi.,Tamura, Toshiki. and Asakura, Tetsuo., Improving cell-adhesive properties ofrecombinant Bombyx mori silk by incorporation of collagen or fibronectinderived peptides produced by transgenic silkworms, Biomacromolecules, 8-11,3487-3492, 2007.
  3. Kino,Rikako., Ikorna, Toshiyuki., Yunoki, Shunji., Nagai, Nobuhiro, Tanaka, Junzo.,Asakura, Tetsuo. and Munekata, Masanobu., Preparation and characterization of multilayeredhydroxyapatite/silk fibroin film,J Biosci Bioeng, 103-6, 514-520, 2007.
  4. Suzuki,Yu., Okonogi, Michi., Yamauchi, Kazuo., Kurosu, Hiromichi., Tansho, Masataka.,Shimizu, Tadashi., Saito, Hazime. and Asakura, Tetsuo., High-field 1HMAS and 15N CP-MAS NMR studies of alanine tripeptides and oligomers:Distinction of antiparallel and parallel beta-sheet structures and twocrystallographically independent molecules, J. Phys. Chem. B, 111-30,9172-9178, 2007.
  5. Asakura,Tetsuo., Sato, Hirohiko., Moro, Fumika., Nakazawa, Yasumoto. and Aoki, Akira,Lamellar structure in Poly(Ala-Gly)determined by solid-state NMR and statistical mechanical calculations, J.Am. Chem. Soc., 129-17, 5703-5709, 2007.
  6. Terry,Gullion., Yamauchi, Kazuo., Okonogi, Michi. and Asakura, Tetsuo., 13C-17OREAPDOR NMR as a tool for determining secondary structure in polyamides,Macromolecules, 40-5, 1363-1365, 2007.
  7. Teramoto,Hidetoshi., Kakazu, Aya., Yamauchi, Kazuo. and Asakura, Tetsuo., Role ofhydroxyl side chains in Bombyx mori silk sericin in stabilizing itssolid structure, Macromolecules, 40-5, 1562-1569, 2007.
  8. Asakura,Tetsuo., Sato, Hirohiko., Moro, Fumika., Yang, Mingying., Nakazawa, Yasumoto.,Collins, Andrew M. and Knight, David P., Solid-state NMR analysis of (GA)3S(AG)3D(GA)3S(AG)3D(GA)3S(AG)3,a peptide with a lamellar structure and a calcium binding site, and productionof TS[(AG)3D(GA)3S]16in Escherichia coli, Macromolecules, 40-25, 8983-8990, 2007.
  9. Asakura,Tetsuo., Yao, Juming., Yang, Mingying., Zhu, Zhenghua. and Hirose, Haruko.,Structure of the spinning apparatus of a wild silkworm Samia cynthia riciniand molecular dynamics calculation on the structural change of the silk fibroin,Polymer, 48-7, 2064-2070, 2007.
  10. Hatae,Shinji., Asakura, Tetsuo. and Fukushima, Yasumasa., Biosynthesis andcharacterization of the artificial protein consisting of marine mussel adhesiveprotein and silk-like protein sequences, Polym. J, 39-4, 294-295, 2007.
  11. Asakura,Tetsuo., Dohi, H., Kimura, H., Kotani, M., Matsunaga, T., Yamauchi, K. andKaji, H., Characterization of molecular orientation of stretched natural rubberby solid-state C-13 NMR, Polym. J, 39-6, 502-503, 2007.
  12. Yang, Mingying., Yamauchi, Kazuo., Kurokawa, Masato. and Asakura, Tetsuo., Design ofsilk-like biomaterials inspired by mussel-adhesive protein, Tissue Eng.,13-12, 2941-2947, 2007.
  13. 朝倉哲郎, フィブロインの高次構造, 蚕糸・昆虫バイオテック, 76-1, 9-14, 2007.
  14. 朝倉哲郎, 未来材料「絹構造の改変と再生医療分野への応用」, ㈱エヌ・ティー・エス, 7-1, 38-44, 2007.
  15. Asakura, Tetsuo., Nakazawa, Yasumoto., Structural analysis ofsilk and application of silk to Biomaterials. Sen-I Gakkaishi, 63-9, 261-265, 2007.
  16. 朝倉哲郎, 日本絹の里紀要「シルクの構造を変える」, 日本絹の里, 10, 61-69, 2007.



2008
  1. Yang,Mingying., Muto, Tomoko., Knight, David P., Collins, Andrew M. and Asakura,Tetsuo., Synthesis and characterization of silklike materials containing thecalcium-binding sequence from calbindin D9k or the shell nacreous matrixprotein MS160, Biomacromolecules, 9-1, 416-420, 2008.
  2. Kumashiro,Kristin K., Ohgo, Kosuke., Niemczura, Walter P., Onizuka, Allen K. and Asakura,Tetsuo., Structural insights into the elastin mimetic (LGGVG)6using solid-state 13C NMR experiments and statistical analysis ofthe PDB, Biopolymers, 89-8, 668-679, 2008.
  3. Zhu,Zhenghua., Ohgo, Kosuke. and Asakura, Tetsuo., Preparation and characterizationof regenerated Bombyx mori silk fibroin fiber with high strength, ExpressPolym Lett, 2-12, 885-889, 2008.
  4. Yang,Mingying, Tanaka, Chikako., Yamauchi, Kazuo., Ohgo, Kosuke., Kurokawa, Masato.and Asakura, Tetsuo., Silklike materials constructed from sequences ofBombyx mori silk fibroin, fibronectin, and elastin, J Biomed Mater Res A,84A-2, 353-363, 2008.
  5. Zhu,Zhenghua., Ohgo, Kosuke., Watanabe, Reiko., Takezawa, Toshiaki. and Asakura,Tetsuo., Preparation and characterization of regenerated Bombyx mori silkfibroin fiber containing recombinant cell-adhesive proteins; Nonwoven fiber andmonofilament, J. Appl. Polym. Sci, 109-5, 2956-2963, 2008.
  6. Yamauchi,Kazuo., Okonogi, Michi., Kurosu, Hiromichi., Tansho, Masataka., Shimizu,Tadashi., Terry, Gullion. and Asakura, Tetsuo., High field 17Osolid-state NMR study of alanine tripeptides, J Magn Reson, 190-2,327-332, 2008.
  7. Ohgo,Kosuke., Bagusat, Frank., Asakura, Tetsuo. and Scheler, Ulrich., Investigationof structural transition of regenerated silk fibroin aqueous solution byRheo-NMR Spectroscopy, J. Am. Chem. Soc., 130-12, 4182-4186, 2008.
  8. Tanaka,Chikako., Takahashi, Rui., Asano, Atsushi., Kurotsu, Takuzo., Akai, Hiromu.,Sato, Kazuhiko., Knight, David P. and Asakura, Tetsuo., Structural analyses ofAnaphe silk fibroin and several model peptides using 13C NMR andX-ray diffraction methods, Macromolecules, 41-3, 796-803, 2008.
  9. Moriya,Motoaki., Ohgo, Kosuke., Masubuchi, Yuichi. and Asakura, Tetsuo., Flow analysisof aqueous solution of silk fibroin in the spinneret of Bombyx morisilkworm by combination of viscosity measurement and finite element methodcalculation, Polymer, 49-4, 952-956, 2008.
  10. Moriya,Motoaki., Ohgo, Kosuke., Masubuchi, Yuichi., Knight, David P. and Asakura,Tetsuo., Micro-computerized tomographic observation of the spinning apparatusin Bombyx mori silkworms, Polymer, 49-26, 5665-5669, 2008.
  11. Sekine,Sokei., Akieda, Hideyuki., Ando, Isao. and Asakura, Tetsuo., A study of therelationship between the tensile strength and dynamics of as-spun and drawnpoly (glycolicacid) fibers, Polym. J, 40-1, 10-16, 2008.
  12. Sato,Hirohiko., Kizuka, Mitsuko., Nakazawa, Yasumoto. and Asakura, Tetsuo., Theinfluence of ser and tyr residues on the structure of Bombyx mori silkfibroin studied using high-resolution solid-state 13C NMRspectroscopy and 13C selectively labeled model peptides, Polym. J,40-3, 184-185, 2008.



2009
  1. Tanaka,Chikako. and Asakura, Tetsuo., Synthesis and Characterization of Cell-AdhesiveSilk-Like Proteins Constructed from the Sequences of Anaphe Silk Fibroin andFibronectin, Biomacromolecules, 10-4, 923-928, 2009.
  2. Moriya,Motoaki., Roschzttardtz, Frederico., Nakahara, Yusuke., Saito, Hitoshi.,Masubuchi, Yuichi. and Asakura, Tetsuo., Rheological Properties of Native SilkFibroins from Domestic and Wild Silkworms, and Flow Analysis in Each Spinneretby a Finite Element Method, Biomacromolecules, 10-4, 929-935, 2009.
  3. Yamaguchi,Erika., Yamauchi, Kazuo., Terry, Gullion. and Asakura, Tetsuo., Structuralanalysis of the Gly-rich region in spider dragline silk using stable-isotopelabeled sequential model peptides and solid-state NMR, Chem. Commun,4176-4178, 2009.
  4. Nakazawa,Yasumoto., Suzuki, Yu., Williamson, Michael P., Saito, Hazime. and Asakura,Tetsuo., The interaction of amyloid A β(1-40) with lipidbilayers and ganglioside as studied by 31P solid-state NMR, Chem.Phys. Lipids, 158-1, 54-60, 2009.
  5. Makaya,Kumiko., Terada, Shinichi., Ohgo, Kosuke. and Asakura, Tetsuo., Comparativestudy of silk fibroin porous scaffolds derived from salt/water and sucrose/hexafluoroisopropanolin cartilage formation, J Biosci Bioeng, 108-1, 68-75, 2009.
  6. Suzuki,Yu., Takahashi, Rui., Shimizu, Tadashi., Tansho, Masataka., Yamauchi, Kazuo.,Williamson, Michael P. and Asakura, Tetsuo., Intra- and Intermolecular Effectson 1H Chemical Shifts in a Silk Model Peptide Determined byHigh-Field Solid State 1H NMR and Empirical Calculations, J.Phys. Chem. B, 113-29, 9756-9761, 2009.
  7. Nagano,Aya., Kikuchi, Yuka., Sato, Hirohiko., Nakazawa, Yasumoto. and Asakura,Tetsuo., Structural Characterization of Silk-Based Water-Soluble Peptides (Glu)n(Ala-Gly-Ser-Gly-Ala-Gly)4(n =4-8) as a Mimic of Bombyx mori Silk Fibroin by 13CSolid-State NMR, Macromolecules, 42-22, 8950-8958, 2009.
  8. Zhu,Zhenghua., Imada, Takuzo. and Asakura, Tetsuo., Preparation andcharacterization of regenerated fiber from the aqueous solution of Bombyxmori cocoon silk fibroin,Mater. Chem. Phys, 117-2-3, 430-433, 2009.
  9. Yang,Mingying., Kawamura, Junji., Zhu, Zhenghua., Yamauchi, Kazuo. and Asakura,Tetsuo., Development of silk-like materials based on Bombyx mori and Nephilaclavipes dragline silk fibroins, Polymer, 50-1, 117-124, 2009.
  10. Sekine,Sokei., Yamauchi, Kazuo., Aoki, Akihiro. and Asakura, Tetsuo., Heterogeneousstructure of poly(glycolic acid) fiber studied withdifferential scanning calorimeter, X-ray diffraction, solid-state NMR andmolecular dynamic simulation, Polymer, 50-25, 6083-6090, 2009.
  11. Tanaka,Chikako., Asano, Atsushi., Kurotsu, Takuzo. and Asakura, Tetsuo., StructuralStudy of Silk-like Peptides Modified by the Addition of the Cell AdhesiveSequence, RGD, Using 13C CP/MAS NMR, Polym. J, 41-1, 18-19,2009.
  12. Sekine, Sokei., Sakiyama, Wataru, Yamauchi, Kazuo. and Asakura, Tetsuo., Detection ofPoorly-Oriented Component in Uniaxially Stretched Poly(glycolicacid) Fiber Studied Using 13C Solid-State NMR, Polym. J, 41-8,582-583, 2009.
  13. Nakazawa,Yasumoto., Asakura, Tetsuo., Development of the Tissue Engineered Medical Products Based onSilk Fibroin from Bombyx mori and Transgenic Silkworm. Sen-I Gakkaishi(レビュー), 65-1, 11-13, 2009.
  14. 朝倉哲郎, 「遺伝子組換えカイコによる蛍光色を持つ高機能絹糸の開発」農林水産技術研究ジャーナル(レビュー), 32-3, 7-10, 2009.
  15. 朝倉哲郎, 「新しいシルクの生産と再生医療材料への応用」工業材料(レビュー), 57-6, 20-23, 2009.
  16. 朝倉哲郎, 「絹の精密構造と再生医療材料の開発」, (財)山田科学振興財団, 財団ニュース平成21年度第1号(レビュー), 6, 2009.
  17. 朝倉哲郎, 「生体との適合性を高めた絹糸の作製と再生医療分野への応用」ブレインテクノニュース(レビュー), 134, 1-6, 2009.
  18. 朝倉哲郎, 「絹繊維化の仕組みを解明 新しい絹を設計, 生産, 再生医療に用いる」, (財)渋沢栄一記念財団(レビュー), 青淵8月号, 16-18, 2009.
  19. 朝倉哲郎, 松田裕生, 「溶液NMR」 高分子分析入門 第Ⅱ部 3章1節, 講談社サイエンティフィック(著書・分担), 122-141, 2009.
  20. 松尾義之, 中澤靖元, 朝倉哲郎, 「シルクの新しい応用分野をひらけ」産官学連携ジャーナルNo.7, 2009.